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Determination of Sulfuric Acid Concentration by Titration

Chemistry | Analytical Chemistry

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Determination of Sulfuric Acid Concentration by Titration

General Aim of Sulfuric Acid Concentration Measurement

Determine the sulfuric acid concentration measurement.

 

Method

Acid-base Titration

Learning Objectives (ILOs)

  • By the of the sulphuric acid experiment, student will:

  • Determine the sulfuric acid concentration measurement .

  • Acquire the correct technique of sulfuric acid titration.

  • Carry out an acid-base titration using phenolphthalein as indicator for sulfuric acid concentration measurement.

Theoretical Background / Context

  • Sample is a solution of unknown concentration.
  • Standard is a solution of exactly known concentration.

Requirements of titrimetric reactions:

  1. The reaction must be simple and expressed by a chemical equation.
  2. A single reaction must occur between the sample and titrant.
  3. The reaction must be instantaneous (rapid).
  4. A suitable standard solution must be available.
  5. The end point should be easily detected.

Types of quantitative reactions:

  1. Neutralization reactions 
  2. H2O formation.
  1. Displacement: Formation of weak acid or weak base.
  1. Complexometric reactions.
  2. Redox reactions (Electron transfer).
  3. Preciptimetric reactions.
 

Principle of Work Assay of Sulphuric Acid

In H2SO4 concentration determination experiment:

  • Sulphuric acid  is a strong acid which can be determined directly using a strong base in the presence of any pH indicator to test for sulphuric acid and sulfuric acid concentration measurement.
  • This determination of sulfuric acid concentration by titration involves measuring the molarity of concentrated H2SO4 or molarity of concentrated sulphuric acid through accurate sulfuric acid concentration measurement techniques.
  • The Sulphuric Acid Purity Test is an analytical procedure used to determine the concentration and purity of sulphuric acid by titration with a standard alkali solution.

H2SO4 +NaOH    Na2SO4 + H2O

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